3-(4-氯苯基)苯丙酮合成路线 （共 35 条）
反应条件
potassium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane
T=80°C; 40 h;
参考文献
Cho, Chan Sik; Shim, Sang Chul
Journal of Organometallic Chemistry, 2006 , vol. 691, # 20 p. 4329 - 4332
反应条件
sodium tetrahydroborate; nickel dichloride in methanol
T=20°C; 0.25 h;
参考文献
Khurana, Jitender M.; Kandpal, Bhaskar M.; Kukreja, Gagan; Sharma, Purnima
Canadian Journal of Chemistry, 2006 , vol. 84, # 8 p. 1019 - 1023
反应条件
ammonium chloride; zinc in tetrahydrofuran
T=20°C; 4 h;
参考文献
Kumar, Anil; Kumar, Satish; Kapoor, Kamal K.
Australian Journal of Chemistry, 2007 , vol. 60, # 8 p. 621 - 623
反应条件
C44H35ClO4P2Ru; potassium hydroxide in para-xylene
T=130°C; 24 h; Inert atmosphereSchlenk techniqueMolecular sieve; Reagent/catalyst;
参考文献
Musa, Sanaa; Ackermann, Lutz; Gelman, Dmitri
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 3077 - 3080
反应条件
sodium hydrogen telluride; 18-crown-6 ether in tetrahydrofuran; ethanol
Ambient temperature;
参考文献
Huang, Xian; Pi, Jin-Hong
Synthetic Communications, 1990 , vol. 20, # 15 p. 2297 - 2300
反应条件
samarium; mercury dichloride in tetrahydrofuran; water
T=20°C; Desulfonylation;
参考文献
Guo, Hongyun; Zhang, Yongmin
Synthetic Communications, 2000 , vol. 30, # 14 p. 2559 - 2564
反应条件
samarium; mercury dichloride in tetrahydrofuran; water
T=20°C; Desulfonylation;
参考文献
Guo, Hongyun; Zhang, Yongmin
Synthetic Communications, 2000 , vol. 30, # 14 p. 2559 - 2564
反应条件
sodium hydrogen telluride in ethanol; N,N-dimethyl-formamide
3 h; Ambient temperature;
参考文献
Huang, Xian; Zhang, Han-zhong
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 97 - 106
反应条件
1: 2-phenoxy-1-phenylethanol With tris(triphenylphosphine)ruthenium(II) chloride; potassium 2-methyl-2-butoxide; ethyl acetate in toluene
T=140°C; 8 h; Schlenk techniqueSealed tubeInert atmosphere;
2: 4-chloro-1-hydroxymethyl-benzene With potassium hydroxide in toluene
T=140°C; 16 h; Schlenk techniqueSealed tubeInert atmosphere;
参考文献
Weickmann, Daniel; Plietker, Bernd
ChemCatChem, 2013 , vol. 5, # 8 p. 2170 - 2173
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine
T=80°C; P=15001.5 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
Sauthier, Mathieu; Lamotte, Nicolas; Dheur, Julien; Castanet, Yves; Mortreux, Andre
New Journal of Chemistry, 2009 , vol. 33, # 5 p. 969 - 971
