反应条件
1: 1.) 100percent xcess nitric acid; 2.) potassium hydroxide / 1.) acetic anhydride, heating, 5h; 2.) methanol, heating, 0.5h
2: 66 percent / sodium nitrite / acetic acid / 1 h / 30 - 70 °C
View Scheme
参考文献
Kyziol, Janusz B.; Daszkiewicz, Zdzislaw
Tetrahedron, 1984 , vol. 40, # 10 p. 1857 - 1862