N-(2-溴乙基)邻苯二甲酰亚胺合成路线 (共 110 条)
反应条件
in N,N-dimethyl-formamide
参考文献
Synthetic Communications, , vol. 15, # 9 p. 837 - 842
参考文献
Chemische Berichte, , vol. 84, p. 254,256
反应条件
sodium hydride 1.) DMF, 0 deg C, 2.) DMF, 20 deg C, 3 h; Yield given. Multistep reaction. Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1837 - 1844
反应条件
sodium hydride 1.) DMF, 0 deg C, 2.) DMF, 20 deg C, 3 h; Yield given. Multistep reaction. Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1837 - 1844
反应条件
T=800°C; P=0.001 Torr; 2 h;
参考文献
Chemische Berichte, , vol. 119, # 7 p. 2387 - 2392
反应条件
potassium hydroxide in water 0.0333333 h; Heating;
参考文献
Ganin, E. V.; Makarov, V. F.; Zakharova, R. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 9 p. 1769 - 1771
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 9 p. 1932 - 1935
反应条件
(i), (ii) N2H4, EtOH; Multistep reaction;
参考文献
Pasini,C. et al.
Farmaco, Edizione Scientifica, 1965 , vol. 20, p. 673 - 685
反应条件
1: 68 percent / C5H11ONa / pentan-1-ol / 8 h / 130 °C 2: 80 percent / H2 / Raney nickel / bis-(2-methoxy-ethyl) ether / 0.5 h / 100 °C / 76000 Torr View Scheme
参考文献
Gordeev, E. N.; Buyanov, V. N.; Zhigachev, V. E.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 1 p. 40 - 42
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 1 p. 46 - 48
反应条件
ethanol; hydrazine hydrate anschliessendes Kochen mit wss.HCl;
参考文献
Michels; Gever
Journal of the American Chemical Society, 1956 , vol. 78, p. 5349
反应条件
2: ethanolic sodium ethylate 3: water; hydrochloric acid View Scheme
参考文献
Koermendy
Acta Chimica Academiae Scientiarum Hungaricae, 1958 , vol. 17, p. 255,261