N-(2-溴乙基)邻苯二甲酰亚胺合成路线 (共 110 条)
反应条件
1: 56 percent / C5H11ONa / pentan-1-ol / 8 h / 130 °C 2: 94 percent / H2 / Raney nickel / bis-(2-methoxy-ethyl) ether / 0.5 h / 100 °C / 76000 Torr View Scheme
参考文献
Ashley et al.
Journal of the Chemical Society, 1959 , p. 3880,3882
参考文献
Adir et Compagnie
Patent: US5332741 A1, 1994 ;
US 5332741 A
反应条件
1-phenyl-1-propyne; Cu in tetrahydrofuran T=25°C; 3 h; Schlenk techniqueGlovebox;
参考文献
Kim, Ju Hyun; Chung, Young Keun
Chemical Communications, 2013 , vol. 49, # 94 p. 11101 - 11103
参考文献
Journal of the Chemical Society, , p. 270,272
参考文献
Chemische Berichte, , vol. 21, p. 571
Chemische Berichte, , vol. 38, p. 2398
反应条件
und Abspaltung von Phthalsaeure aus dem Reaktionsprodukt;
参考文献
I.G. Farbenind.
Patent: DE498661 , 1928 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 2450
反应条件
(i), (ii) N2H4, EtOH; Multistep reaction;
参考文献
Pasini,C. et al.
Farmaco, Edizione Scientifica, 1965 , vol. 20, p. 673 - 685
反应条件
1: 54 percent / tetrahydrofuran; cyclohexane; diethyl ether / -40 deg C, 40 min, room temp., 17 h 2: 49 percent / hydrazine hydrate / dimethylformamide / 20 h / Heating View Scheme
参考文献
Wharton, Clifford J.; Wrigglesworth, Roger
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 809 - 814
反应条件
T=100°C; Zersetzen das Produkt durch Kochen mit Salzsaeure von 20prozent;
参考文献
Chemische Berichte, , vol. 29, p. 2530
反应条件
potassium carbonate in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Societe Anonyme dite: L'OREAL
Patent: US4337061 A1, 1982 ;