alpha-巯基苯丙烯酸合成路线 （共 11 条）
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2417 - 2424
反应条件
1: alcohol; hydroxylamine 2: sodium amalgam; lactic acid; absolute alcohol View Scheme
参考文献
Graenacher
Helvetica Chimica Acta, 1922 , vol. 5, p. 614,619
参考文献
Graenacher
Helvetica Chimica Acta, 1922 , vol. 5, p. 614,619
反应条件
1: With sodium acetate; acetic anhydride
T=100°C; 1 h; Inert atmosphere;
2: With sodium hydroxide; water
T=75°C; 2 h; Inert atmosphere;
参考文献
Inamoto, Kiyofumi; Arai, Yukari; Hiroya, Kou; Doi, Takayuki
Chemical Communications, 2008 , # 43 p. 5529 - 5531
反应条件
sodium hydroxide in water
T=80 - 90°C; Inert atmosphere;
参考文献
Kottakota, Suresh K.; Benton, Mathew; Evangelopoulos, Dimitrios; Guzman, Juan D.; Bhakta, Sanjib; McHugh, Timothy D.; Gray, Mark; Groundwater, Paul W.; Marrs, Emma C. L.; Perry, John D.; Harburn, J. Jonathan
Organic Letters, 2012 , vol. 14, # 24 p. 6310 - 6313
反应条件
aluminum oxide; sodium hydroxide in solid
0.0833333 h; microwaves (210 W);
参考文献
Villemin, Didier; Alloum, Abdelkrim Ben
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 79, # 1,4 p. 33 - 42
反应条件
1: ammonium acetate / toluene / 90 - 100 °C / |Inert atmosphere
2: sodium hydroxide / water / 80 - 90 °C / |Inert atmosphere
View Scheme
参考文献
Kottakota, Suresh K.; Benton, Mathew; Evangelopoulos, Dimitrios; Guzman, Juan D.; Bhakta, Sanjib; McHugh, Timothy D.; Gray, Mark; Groundwater, Paul W.; Marrs, Emma C. L.; Perry, John D.; Harburn, J. Jonathan
Organic Letters, 2012 , vol. 14, # 24 p. 6310 - 6313
反应条件
1: 67 percent / conc. HCl / ethanol / Heating
2: 15 percent / 5percent KOH / H2O / Heating
View Scheme
参考文献
Pavlenko, N. I.; Marshtupa, V. P.; Klyuev, N. A.; Baskunov, B. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 8 p. 808 - 812
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , # 8 p. 1088 - 1093
反应条件
potassium hydroxide in water
Heating;
参考文献
Pavlenko, N. I.; Marshtupa, V. P.; Klyuev, N. A.; Baskunov, B. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 8 p. 808 - 812
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , # 8 p. 1088 - 1093
参考文献
Ginsburg; Bondzynski
Chemische Berichte, 1886 , vol. 19, p. 114,117
Full Text Show Details
Bondzynski
Monatshefte fuer Chemie, 1887 , vol. 8, p. 350
