in not given
n-BuMgCl reacted with GeCl4; reduced with LiAlH4; purified by trap to trap distn.;
参考文献
Laplante, Arthur J.; Stidham, Howard D.; Peebles, Sean A.; Peebles, Rebecca A.; Wurrey, Charles J.; Guirgis, Gamil A.
Journal of Molecular Structure, 2011 , vol. 985, # 1 p. 5 - 13