2-甲氧基-4-甲基苯甲醛合成路线 （共 12 条）
反应条件
dipyridinium dichromate in dichloromethane 51 h; Ambient temperature;
参考文献
Glennon, Richard A.; Raghupathi, Reva; Bartyzel, Piotr; Teitler, Milt; Leonhardt, Sigrun
Journal of Medicinal Chemistry, 1992 , vol. 35, # 4 p. 734 - 740
反应条件
dipotassium peroxodisulfate; copper(II) sulfate in water; acetonitrile Heating;
参考文献
Hauser, Frank M.; Ellenberger, Suzanne R.
Synthesis, 1987 , # 8 p. 723 - 724
反应条件
1: triethylamine / CH2Cl2 / 4 h / Ambient temperature 2: sodium hydride / tetrahydrofuran / 18 h / Heating 3: 1.) potassiun, tert-butyl alcohol, ammonia / 1.) THF, -78 deg C, 2.) THF, -78 deg C, 1 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, p. 7828
反应条件
1: sodium hydride / tetrahydrofuran / 18 h / Heating 2: 1.) potassiun, tert-butyl alcohol, ammonia / 1.) THF, -78 deg C, 2.) THF, -78 deg C, 1 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, p. 7828
反应条件
1: 63 percent / LiAlH4 / tetrahydrofuran / 1.) reflux, 25.5 h, 2.) RT, 91 h 2: 59 percent / pyridinium dichromate / CH2Cl2 / 51 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 4 p. 734 - 740
反应条件
ammonia; potassium; tert-butyl alcohol 1.) THF, -78 deg C, 2.) THF, -78 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 110, p. 7828
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 35, p. 142
参考文献
Chuit; Bolsing
Bulletin de la Societe Chimique de France, 1906 , vol. <3> 35, p. 142
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 10 h; Inert atmosphere;
参考文献
Gensini, Martina; Altamura, Maria; Dimoulas, Tula; Fedi, Valentina; Giannotti, Danilo; Giuliani, Sandro; Guidi, Antonio; Harmat, Nicholas J. S.; Meini, Stefania; Nannicini, Rossano; Pasqui, Franco; Tramontana, Manuela; Triolo, Antonio; Maggi, Carlo Alberto
ChemMedChem, 2010 , vol. 5, # 1 p. 65 - 78
反应条件
sodium chlorite; aminosulfonic acid in tetrahydrofuran; water Ambient temperature;
参考文献
Hauser, Frank M.; Ellenberger, Suzanne R.
Synthesis, 1987 , # 8 p. 723 - 724
