hydrogen; palladium on activated charcoal in methanol T=80°C; P=2585.7 Torr; 20 h;

1: 1.) aq. NaOH / 1.) 10-15 deg C, 2.) 95 deg C, 2 h 2: 68 percent / H2 / 5percent Pd/C / methanol / 20 h / 80 °C / 2585.7 Torr View Scheme