T=100 - 150°C;

C13H13IrN4O5(2+)*O4S(2-); potassium hydrogencarbonate; deuterium in water T=50°C; P=7500.75 Torr; 1 h;

C21H36Cl2IrN2; potassium hydroxide in water-d2 T=110°C; P=38002.6 Torr; Autoclave;

NaOD in water-d2 175 deg C, 445 psi, 6 h, 175 deg C to RT, 18 h;

potassium carbonate T=100°C; 3 h;

(2,6-bis(diisopropylphosphinomethyl)pyridine)iridium(III)trihydride in tetrahydrofuran; water-d2 Kinetics; High Pressure; mixt. of Ir complex and soln. of KOH in D2O placed in stainless autoclave; pressurized by equimolar mixt. of CO2 and H2; heated to 200°C (oil bath); stirred for 2 h; not isolated; detd. by (2)H NMR spectra;