air in tetrahydrofuran byproducts: cyclohexane; N2-atmosphere; treatment of B2H6 with olefin, addn. of MeSH (stirring), injecting small amt. of air (in two steps during 2 h), stirring for 12 h; evapn. of volatiles (reduced pressure), fractional distn. (reduced pressure);

暂无反应条件数据

(i) B2H6, Et2O, (ii) /BRN= 906737/; Multistep reaction;