4,6-二苯基-[2,2]联吡啶合成路线 （共 17 条）
反应条件
ammonium acetate in acetic acid
2 h; Heating;
参考文献
Cave, Gareth W. V.; Raston, Colin L.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 24 p. 3258 - 3264
反应条件
1: NaOH / 0.17 h
2: 2.66 g / NH4OAc / acetic acid / 2 h / Heating
View Scheme
参考文献
Cave, Gareth W. V.; Raston, Colin L.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 24 p. 3258 - 3264
反应条件
1: 25 percent / BF3-OEt2 / 0.5 h / 100 °C
2: NH3 / ethanol / 0.5 h
View Scheme
参考文献
Katritzky, Alan R.; Elisseou, E. Michael; Patel, Ranjan C.; Plau, Bernard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 125 - 130
反应条件
1: BF3-Et2O
2: NH3 / ethanol / 0.5 h
View Scheme
参考文献
Katritzky, Alan R.; Elisseou, E. Michael; Patel, Ranjan C.; Plau, Bernard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 125 - 130
反应条件
1: BF3-Et2O
2: NH3 / ethanol / 0.5 h
View Scheme
参考文献
Katritzky, Alan R.; Elisseou, E. Michael; Patel, Ranjan C.; Plau, Bernard
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 125 - 130
反应条件
1: [Rh(OH)(cycloocta-1,5-diene)]2; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl / 1,4-dioxane; water / 12 h / 75 °C / Inert atmosphere
2: sodium hydroxide / 1,4-dioxane / 2.5 h / 75 °C
View Scheme
参考文献
Lau, Chan; Tsui, Gavin Chit; Lautens, Mark
Synthesis, 2011 , # 23 art. no. Z92211SS, p. 3908 - 3914
反应条件
in ethanol
3 h; Reflux;
参考文献
Constable, Edwin C.; Housecroft, Catherine E.; Kopecky, Peter; Martin, Colin J.; Wright, Iain A.; Zampese, Jennifer A.; Bolink, Henk J.; Pertegas, Antonio
Dalton Transactions, 2013 , vol. 42, # 22 p. 8086 - 8103
