tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide 4 h; electrochemical reduction; Yields of byproduct given;
参考文献
Grimshaw, James; Hamilton, Robert; Trocha-Grimshaw, Jadwiga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 229 - 234
1: 1.6 g / hydrazine hydrate / 5percent Pd/C / ethanol / 2 h / Heating
2: 2.7 g / pyridine / 3 h / Ambient temperature
3: 0.8 g / 2-chlorobenzoyl chloride / 3 h / 200 °C
View Scheme
参考文献
Grimshaw, James; Hamilton, Robert; Trocha-Grimshaw, Jadwiga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 229 - 234
Grimshaw, James; Hamilton, Robert; Trocha-Grimshaw, Jadwiga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 229 - 234
1: 72 h / 180 °C
2: 0.1 tetrapropylammoniun fluoroborate / dimethylformamide / 4 h / electrochemical reduction
View Scheme
参考文献
Grimshaw, James; Hamilton, Robert; Trocha-Grimshaw, Jadwiga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 229 - 234
1: 72 h / 180 °C
2: 0.1 tetrapropylammoniun fluoroborate / dimethylformamide / 4 h / electrochemical reduction
View Scheme
参考文献
Grimshaw, James; Hamilton, Robert; Trocha-Grimshaw, Jadwiga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 229 - 234
1: 2.7 g / pyridine / 3 h / Ambient temperature
2: 0.8 g / 2-chlorobenzoyl chloride / 3 h / 200 °C
View Scheme
参考文献
Grimshaw, James; Hamilton, Robert; Trocha-Grimshaw, Jadwiga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 229 - 234
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide
4 h; electrochemical reduction; Yields of byproduct given;
参考文献
Grimshaw, James; Hamilton, Robert; Trocha-Grimshaw, Jadwiga
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 229 - 234