(+)-顺式-1(r),2(s)-1,2-二羟基-1,2,3,4-四氢萘合成路线 （共 4 条）
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; AZADO; tetrabutylammomium bromide in water; acetonitrile T=0 - 20°C; 4 h; Inert atmosphere;
参考文献
Shibuya, Masatoshi; Shibuta, Takuro; Fukuda, Hayato; Iwabuchi, Yoshiharu
Organic Letters, 2012 , vol. 14, # 19 p. 5010 - 5013
反应条件
AZADO; [bis(acetoxy)iodo]benzene; tetrabutylammomium bromide in water; acetonitrile T=0 - 20°C; 4 h; Inert atmosphere;
参考文献
Shibuya, Masatoshi; Shibuta, Takuro; Fukuda, Hayato; Iwabuchi, Yoshiharu
Organic Letters, 2012 , vol. 14, # 19 p. 5010 - 5013
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; AZADO; tetrabutylammomium bromide in water; acetonitrile T=0 - 20°C; 4 h; Inert atmosphere;
参考文献
Shibuya, Masatoshi; Shibuta, Takuro; Fukuda, Hayato; Iwabuchi, Yoshiharu
Organic Letters, 2012 , vol. 14, # 19 p. 5010 - 5013
反应条件
1: With 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; AZADO; tetrabutylammomium bromide in water; acetonitrile
T=0 - 20°C; 4 h; Inert atmosphere;
2: With diazomethane in water; acetonitrile
T=0 - 20°C; 4 h; Inert atmosphere;
参考文献
Shibuya, Masatoshi; Shibuta, Takuro; Fukuda, Hayato; Iwabuchi, Yoshiharu
Organic Letters, 2012 , vol. 14, # 19 p. 5010 - 5013
