(2R,2'R,3S,3'S,4S)-2,2'-二(3,4-二羟基苯基)-3,3',4,4'-四氢-[4,8'-联-2H-1-苯并吡喃]-3,3',5',7,7'-五醇合成路线 （共 3 条）
57526-59-7(2R,2'R,3S,3'S,4S)-2,2'-二(3,4-二羟基苯基)-3,3',4,4'-四氢-[4,8'-联-2H-1-苯并吡喃]-3,3',5',7,7'-五醇
→
反应条件
NaBD3CN in trifluoroacetic acid T=0°C; 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 23 p. 3005 - 3012
57526-59-7(2R,2'R,3S,3'S,4S)-2,2'-二(3,4-二羟基苯基)-3,3',4,4'-四氢-[4,8'-联-2H-1-苯并吡喃]-3,3',5',7,7'-五醇
→
反应条件
sodium cyanoborohydride; trifluoroacetic acid T=0°C; 3 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 1 p. 31 - 32
57526-59-7(2R,2'R,3S,3'S,4S)-2,2'-二(3,4-二羟基苯基)-3,3',4,4'-四氢-[4,8'-联-2H-1-苯并吡喃]-3,3',5',7,7'-五醇
→
反应条件
acetic acid; chloroacetic acid in ethanol 24 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2521 - 2528
