1,3-二氯-3-甲基-2-丁酮合成路线 （共 28 条）
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide T=20°C; glassy carbon electrode;
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 2 p. 167 - 175
反应条件
sulfuryl dichloride
T=40 - 50°C; 25 h;
参考文献
Sakai, Takashi; Ishikawa, Mutsumi; Amano, Eiichiro; Utaka, Masanori; Takeda, Akira
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 6 p. 2295 - 2297
反应条件
silver tetrafluoroborate in diethyl ether
T=-20°C;
参考文献
Griesbaum, Karl; Lie, Giu Oan; Raupp, Erwin
Chemische Berichte, 1981 , vol. 114, # 10 p. 3273 - 3280
反应条件
silver tetrafluoroborate in diethyl ether
T=-20°C;
参考文献
Griesbaum, Karl; Lie, Giu Oan; Raupp, Erwin
Chemische Berichte, 1981 , vol. 114, # 10 p. 3273 - 3280
反应条件
1: 27 percent / KOH / 4 h / 150 °C
2: 44 percent / m-chloroperbenzoic acid / CH2Cl2 / 240 h / Ambient temperature
3: 168 h / Ambient temperature
View Scheme
参考文献
Griesbaum, Karl; Lie, Giu Oan; Raupp, Erwin
Chemische Berichte, 1981 , vol. 114, # 10 p. 3273 - 3280
反应条件
1: 1) HCl, 2) Cl2 / 1) -30 to -20 deg C, 5 h, 2) -30 to -20 deg C, 7 h
2: 27 percent / KOH / 4 h / 150 °C
3: 44 percent / m-chloroperbenzoic acid / CH2Cl2 / 240 h / Ambient temperature
4: 168 h / Ambient temperature
View Scheme
参考文献
Griesbaum, Karl; Lie, Giu Oan; Raupp, Erwin
Chemische Berichte, 1981 , vol. 114, # 10 p. 3273 - 3280
反应条件
1: 44 percent / m-chloroperbenzoic acid / CH2Cl2 / 240 h / Ambient temperature
2: 168 h / Ambient temperature
View Scheme
参考文献
Griesbaum, Karl; Lie, Giu Oan; Raupp, Erwin
Chemische Berichte, 1981 , vol. 114, # 10 p. 3273 - 3280
反应条件
1: 0.79 g / m-chloroperbenzoic acid / CH2Cl2 / 72 h / Ambient temperature
2: 168 h / Ambient temperature
View Scheme
参考文献
Griesbaum, Karl; Lie, Giu Oan; Raupp, Erwin
Chemische Berichte, 1981 , vol. 114, # 10 p. 3273 - 3280
反应条件
chlorine in tetrachloromethane
1.) below 40 deg C, 2.) room temperature, 0.5 h; Product distribution;
参考文献
Gallucci, R. R.; Going, R.
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2532 - 2538
反应条件
168 h; Ambient temperature; Yield given;
参考文献
Griesbaum, Karl; Lie, Giu Oan; Raupp, Erwin
Chemische Berichte, 1981 , vol. 114, # 10 p. 3273 - 3280
