2-(2-氨乙基)-1,3-二氧戊环合成路线 (共 6 条)
反应条件
hydrogen; platinum(IV) oxide in ethanol P=2947.7 Torr;
参考文献
Crumbie, Robyn L.; Nimitz, Jonathan S.; Mosher, Harry S.
Journal of Organic Chemistry, 1982 , vol. 47, # 21 p. 4040 - 4045
参考文献
BRACCO S.p.A.; DIBRA S.p.A.
Patent: EP760683 B1, 2000 ;
反应条件
hydrogen; interlamellar montmorillonitediphenyl phosphine palladium(II) in ethanol 0.416667 h; Ambient temperature;
参考文献
Sharma, G. V. M.; Chandrasekhar, S.
Synthetic Communications, 1989 , vol. 19, # 19 p. 3289 - 3294
反应条件
1: 90 percent / sodium azide, tetra-n-hexylammonium bromide / H2O / 2 h 2: 1.) Ph3P, 2.) H2O / 1) THF, 3 h, below 40 deg C, 20 deg C (1 h); 2) 1 h, 20 deg C View Scheme
参考文献
Synthetic Communications, , vol. 17, # 4 p. 377 - 384
参考文献
Journal of Organic Chemistry, , vol. 21, p. 115,116
反应条件
triethylamine T=75°C; 4.5 h;
参考文献
Gribble, Gordon W.; Switzer, Frank L.
Synthetic Communications, 1987 , vol. 17, # 4 p. 377 - 384