5-溴-2-羟基-4-甲氧基苯甲醛合成路线 （共 16 条）
反应条件
1: Methylierung 2: permanganate View Scheme
参考文献
Rao; Srikantia; Iyengar
Journal of the Chemical Society, 1929 , p. 1580
参考文献
Rao; Srikantia; Iyengar
Journal of the Chemical Society, 1929 , p. 1580
反应条件
bromine in dichloromethane
T=-20°C; 0.333333 h; Inert atmosphere; regioselective reaction;
参考文献
Borikar; Daniel
Journal of the Iranian Chemical Society, 2011 , vol. 8, # 2 p. 531 - 536
反应条件
boron trichloride in dichloromethane
T=20°C; 16 h;
参考文献
Cordoba, Ruben; Tormo, Nelida Salvador; Medarde, Antonio Fernandez; Plumet, Joaquin
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 15 p. 5300 - 5315
反应条件
triethylamine; magnesium chloride in tetrahydrofuran
Inert atmosphereReflux; regioselective reaction;
参考文献
Akselsen, yvind W.; Skattebol, Lars; Hansen, Trond Vidar
Tetrahedron Letters, 2009 , vol. 50, # 46 p. 6339 - 6341
反应条件
pyridine; pyridinium hydrobromide perbromide
T=50°C; 2 h;
参考文献
Cordoba, Ruben; Tormo, Nelida Salvador; Medarde, Antonio Fernandez; Plumet, Joaquin
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 15 p. 5300 - 5315
反应条件
sodium dithionite
und Austausch der Aminogruppe gegen Brom;
参考文献
Rao; Srikantia; Iyengar
Journal of the Chemical Society, 1929 , p. 1580
反应条件
1: HCl; diethyl ether / und anschliessend mit H2O
2: K2CO3; benzene
View Scheme
参考文献
Seshadri; Varadarajan
Journal of Scientific and Industrial Research, 1952 , vol. 11 B, p. 39,43
反应条件
1: acetic acid; bromine
2: K2CO3; benzene
View Scheme
参考文献
Seshadri; Varadarajan
Journal of Scientific and Industrial Research, 1952 , vol. 11 B, p. 39,43
反应条件
potassium carbonate; benzene
参考文献
Seshadri; Varadarajan
Journal of Scientific and Industrial Research, 1952 , vol. 11 B, p. 39,43
