7-甲氧基-2H-色烯-3-甲腈合成路线 (共 4 条)
反应条件
1,4-diaza-bicyclo[2.2.2]octane
24 h; Heating;
参考文献
Corey; Wu
Journal of the American Chemical Society, 1993 , vol. 115, # 20 p. 9327 - 9328
反应条件
1: 90 percent / 10percent aq. NaOH / 24 h / Heating
2: (PhO)2P(=O)N3, Et3N / 45 °C
3: 2.) 6N aq. HCl / 1.) toluene, 80 deg C, 2.) reflux
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参考文献
Corey; Wu
Journal of the American Chemical Society, 1993 , vol. 115, # 20 p. 9327 - 9328
反应条件
hydroxylamine hydrochloride; sodium hydrogencarbonate in ethanol; water
3 h; Heating;
参考文献
Riffaud; Dupont; Rene; Royer
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 6 p. 577 - 581
反应条件
sodium hydroxide
24 h; Heating;
参考文献
Corey; Wu
Journal of the American Chemical Society, 1993 , vol. 115, # 20 p. 9327 - 9328