7-苯基-3,4-二氢-1H-1,4-二氮杂革-5(2H)-酮合成路线 （共 4 条）
反应条件
in xylene 1 h; Heating;
参考文献
Chammache, M.; Essassi, E. M.; Salem, M.; Zniber, R.
Bulletin des Societes Chimiques Belges, 1993 , vol. 102, # 2 p. 89 - 98
Title/Abstract Full Text Show Details
Chammache; Zellou; Essassi; Cherrah; Hassar
Annales Pharmaceutiques Francaises, 2001 , vol. 59, # 3 p. 206 - 210
反应条件
1: 90 percent / H2 / Pd/C / methanol / 24 h / 60 °C / 37503 Torr 2: 95 percent / DIEA / dioxane; H2O / 48 h / 20 °C View Scheme
参考文献
Wlodarczyk, Nicolas; Le Broc-Ryckewaert, Delphine; Gilleron, Pauline; Lemoine, Amelie; Farce, Amaury; Chavatte, Philippe; Dubois, Joelle; Pommery, Nicole; Henichart, Jean-Pierre; Furman, Christophe; Millet, Regis
Journal of Medicinal Chemistry, 2011 , vol. 54, # 5 p. 1178 - 1190
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=60°C; P=37503.8 Torr; 24 h; Autoclave;
参考文献
Wlodarczyk, Nicolas; Le Broc-Ryckewaert, Delphine; Gilleron, Pauline; Lemoine, Amelie; Farce, Amaury; Chavatte, Philippe; Dubois, Joelle; Pommery, Nicole; Henichart, Jean-Pierre; Furman, Christophe; Millet, Regis
Journal of Medicinal Chemistry, 2011 , vol. 54, # 5 p. 1178 - 1190
