4-甲氧基-2-硝基溴苄合成路线 （共 15 条）
反应条件
dihydrogen peroxide; bromine in dichloromethane; water 4 h; Reflux;
参考文献
Amati, Alessandro; Dosualdo, Gabriele; Zhao, Lihua; Bravo, Anna; Fontana, Francesca; Minisci, Francesco; Bjorsvik, Hans-Rene
Organic Process Research and Development, 1998 , vol. 2, # 4 p. 261 - 269
反应条件
phosphorus tribromide in diethyl ether 3 h; Inert atmosphere;
参考文献
Kong, Chen; Jana, Navendu; Driver, Tom G.
Organic Letters, 2013 , vol. 15, # 4 p. 824 - 827
反应条件
1: dimethylsulfide borane complex / tetrahydrofuran / 3 h / 80 °C / |Inert atmosphere 2: phosphorus tribromide / diethyl ether / 3 h / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 15, # 4 p. 824 - 827
反应条件
1: (i) HNO3, H2SO4, (ii) aq. NaNO2, (iii) aq. H2SO4 2: aq. NaOH 3: NBS, (PhCO)2O2 / CCl4 / Irradiation View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 91, p. 1152 - 1161
反应条件
1: aq. NaOH 2: NBS, (PhCO)2O2 / CCl4 / Irradiation View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 91, p. 1152 - 1161
反应条件
1: sodium tetrahydroborate / methanol / 1 h / 0 - 5 °C / Inert atmosphere 2: phosphorus tribromide / toluene / 0.5 h / 40 - 100 °C / Inert atmosphere View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 18 p. 6254 - 6276
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 9 p. 2475 - 2480
反应条件
water in acetone 26 h; Reflux;
参考文献
Siles, Rogelio; Ackley, J. Freeland; Hadimani, Mallinath B.; Hall, John J.; Mugabe, Benon E.; Guddneppanavar, Rajsekhar; Monk, Keith A.; Chapuis, Jean-Charles; Pettit, George R.; Chaplin, David J.; Edvardsen, Klaus; Trawick, Mary Lynn; Garner, Charles M.; Pinney, Kevin G.
Journal of Natural Products, 2008 , vol. 71, # 3 p. 313 - 320
反应条件
tetra(n-butyl)ammonium dichromate(VI) in chloroform 0.166667 h; Heating;
参考文献
Katritzky, Alan R.; Xu, Yong-Jiang; Vakulenko, Anatoliy V.; Wilcox, Allan L.; Bley, Keith R.
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 9100 - 9104
反应条件
1: 5 h / Heating 2: 47 percent / NaH / 1,2-dimethoxy-ethane / 2 h / Heating 3: 98 percent / H2, morpholine / 5 percent Rh/C / ethanol; methanol / 4 h / 18100.2 Torr / Ambient temperature 4: 86 percent / HCOONa / 3 h / Heating View Scheme
参考文献
Jorgensen, Tine Krogh; Andersen, Knud Erik; Lau, Jesper; Madsen, Peter; Huusfeldt, Per Olaf
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 1 p. 57 - 64
