2-溴-1,3,5-三甲基苯合成路线 (共 240 条)
反应条件
1: 2-Bromo-1,3,5-trimethyl-benzene With magnesium in tetrahydrofuran Heating; 2: 2-Carboxybenzaldehyde in tetrahydrofuran
参考文献
Mohanakrishnan, Arasambattu K.; Amaladass
Tetrahedron Letters, 2005 , vol. 46, # 24 p. 4225 - 4229
反应条件
1: sodium; benzene 2: diluted nitric acid / 115 - 130 °C / im geschlossenen Rohr View Scheme
参考文献
Chemische Berichte, , vol. 27, p. 3444
Chemische Berichte, , vol. 28, p. 531
反应条件
2-((dicyclohexylphosphino)methyl)-1,3-bis(2,6-diisopropylphenyl)-4,5-dimethyl-1H-imidazol-3-ium iodide; ammonia; palladium diacetate; sodium t-butanolate in 1,4-dioxane T=120°C; P=7500.75 Torr; 24 h; AutoclaveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 35 p. 9599 - 9604
反应条件
ammonia; KNH2 T=-33°C; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 102, # 24 p. 7375 - 7377
反应条件
ammonia; KNH2 T=-33°C; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 102, # 24 p. 7375 - 7377
反应条件
sodium amide in diethyl ether; ammonia 2 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 49, # 19 p. 3584 - 3587
反应条件
ammonia; KNH2 T=-33°C; Product distributionRate constant;
参考文献
Journal of the American Chemical Society, , vol. 102, # 24 p. 7375 - 7377
参考文献
Smith; Moyle
Journal of the American Chemical Society, 1936 , vol. 58, p. 1,9
参考文献
Smith; Moyle
Journal of the American Chemical Society, 1936 , vol. 58, p. 1,9
反应条件
1: magnesium / tetrahydrofuran / 0.33 h / 80 °C / microwave irradiation 2: 74 percent / tetrahydrofuran / 0.08 h / 1 °C View Scheme
参考文献
Khaibulova, T. Sh.; Boyarskaya; Boyarskii
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 3 p. 360 - 365
Zh. Org. Khim., 2013 , vol. 49, # 3 p. 373 - 378