1,14-二溴-3,6,9,12-四恶十四烷合成路线 (共 8 条)
反应条件
bromine; triphenylphosphine in acetonitrile T=20°C; 48 h;
参考文献
Biron, Eric; Otis, Francois; Meillon, Jean-Christophe; Robitaille, Martin; Lamothe, Julie; Van Hove, Patrick; Cormier, Marie-Eve; Voyer, Normand
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 6 p. 1279 - 1290
反应条件
lithium bromide in acetone 20 h; Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 3 p. 557 - 560
Steroids, , vol. 71, # 10 p. 911 - 921
反应条件
lithium bromide in acetone Reflux;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 2 p. 636 - 643
反应条件
sodium bromide; 1,1-dibromomethane in N,N-dimethyl-formamide
参考文献
Canadian Journal of Chemistry, , vol. 66, p. 1097 - 1108
反应条件
1: pyridine / 3 h / 0 - 20 °C 2: lithium bromide / acetone / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 2 p. 636 - 643
反应条件
potassium carbonate in acetonitrile 12 h;
参考文献
Mendeleev Communications, , vol. 17, # 6 p. 330 - 331
反应条件
in N,N-dimethyl-formamide T=20°C; 72 h;
参考文献
Dime, David S.; Backx, Peter; Kimmeldirk, Klaus
Patent: EP966304 B1, 2005 ;
Location in patent: Page/Page column 17 ;
反应条件
in ethanol
5 h; Heating;
参考文献
Bradshaw, Jerald S.; Krakowiak, Krzysztof E.; Izatt, Reed M.; Bruening, Ronald L.; Tarbet, Bryon J.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 347 - 349