triethylamine; (1R,2R,4S,5S)-4,8,8-triMe-2-Ph-2-phosphabicyclo[3.3.0]octane in 1,1-dimethylpropan-1-ol; dichloromethane T=20°C; 3 h; Inert atmosphereResolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Duffey, Trisha A.; MacKay, James A.; Vedejs, Edwin
Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4674 - 4685
triethylamine; C16H23P*BF4(1-)*H(1+) in toluene T=-40°C; 6 h; Inert atmosphereResolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Duffey, Trisha A.; MacKay, James A.; Vedejs, Edwin
Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4674 - 4685
Candida antarctica lipase B in n-heptane T=60°C; 3 h; Microwave irradiationResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Yadav, Ganapati D.; Devendran, Saravanan
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 81, p. 58 - 65
{3-[2-(3,5-dimethylphenyl)naphthalen-1-yl]pyridin-4-yl}diethylamine; triethylamine in toluene T=-78°C; 2 h; optical yield given as percent ee;
参考文献
Larionov, Evgeny; Mahesh, Mohan; Spivey, Alan C.; Wei, Yin; Zipse, Hendrik
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9390 - 9399
