1-苄基-3-甲氧基羰酰-4-哌啶酮合成路线 (共 13 条)
反应条件
1: HCl / 2 h / 70 °C
2: LiAlH4 / diethyl ether / Heating
View Scheme
参考文献
Nagai; Uno; Umemoto
Chemical and Pharmaceutical Bulletin, 1977 , vol. 25, # 8 p. 1911 - 1922
参考文献
Bhisetti, Govinda R.; Saunders, Jeffrey O.; Murcko, Mark A.; Lepre, Christopher A.; Britt, Shawn D.; Come, Jon H.; Deininger, David D.; Wang, Tianshang
Patent: US2003/95958 A1, 2003 ;
US 20030095958 A1
反应条件
1: NaBH4 / methanol / 2 h / 0 - 20 °C
2: triethylamine; MeSO2Cl / CH2Cl2 / 0 - 20 °C
View Scheme
参考文献
Chavan, Subhash P.; Khobragade, Dushant A.; Pathak, Ashok B.; Kalkote, Uttam R.
Synthetic Communications, 2007 , vol. 37, # 18 p. 3143 - 3149