(2,2-二甲基丙基)亚膦酸二氯化物合成路线 （共 3 条）
反应条件
1: With magnesium in diethyl ether; ethylene dibromide
RefluxInert atmosphere;
2: With cadmium (II) chloride in diethyl ether; ethylene dibromide
T=0°C; 2 h; Inert atmosphere;
3: With phosphorus trichoride in diethyl ether; ethylene dibromide
T=0 - 20°C; 3.5 h; Inert atmosphere;
参考文献
Patra, Sanjib K.; Whittell, George R.; Nagiah, Simone; Ho, Cheuk-Lam; Wong, Wai-Yeung; Manners, Ian
Chemistry - A European Journal, 2010 , vol. 16, # 10 p. 3240 - 3250
反应条件
phosphorus trichoride
参考文献
King,R.B. et al.
Journal of Organic Chemistry, 1976 , vol. 41, # 6 p. 972 - 977
反应条件
lithium aluminium tetrahydride
参考文献
King,R.B. et al.
Journal of Organic Chemistry, 1976 , vol. 41, # 6 p. 972 - 977
