2,2-二甲基苯乙酸甲酯合成路线 (共 49 条)
反应条件
2BF4(1+)*C27H50P2*2H(1+); palladium diacetate; caesium carbonate in toluene T=60°C; 14 h; Inert atmosphere;
参考文献
Flores-Gaspar, Areli; Martin, Ruben
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1223 - 1228
反应条件
2BF4(1+)*C27H50P2*2H(1+); palladium diacetate; caesium carbonate in toluene T=60°C; 14 h; Inert atmosphere;
参考文献
Flores-Gaspar, Areli; Martin, Ruben
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1223 - 1228
反应条件
potassium carbonate in dimethyl sulfoxide T=90°C; 16 h; Inert atmosphereGreen chemistry;
参考文献
Ji, Yuan; Sweeney, Jessica; Zoglio, Jillian; Gorin, David J.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11606 - 11611
反应条件
titanium tetraethoxide; tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide electroreduction (lead cathode, carbon rod anode, 4-5 F/mol);
参考文献
Journal of Organic Chemistry, , vol. 55, # 17 p. 5037 - 5041
反应条件
poly[4-(diacetoxyiodo)styrene]; sulfuric acid in acetonitrile T=60°C; 0.5 h;
参考文献
Sheng, Shou-Ri; Zhong, Ming-Hua; Liu, Xiao-Ling; Luo, Qiu-Yan; Chen, Hui-Zong
Journal of Chemical Research, 2004 , # 6 p. 392 - 393
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 12 p. 3939 - 3940
反应条件
2BF4(1+)*C27H50P2*2H(1+); palladium diacetate; caesium carbonate in toluene T=60°C; 14 h; Inert atmosphere;
参考文献
Flores-Gaspar, Areli; Martin, Ruben
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1223 - 1228
反应条件
1: methyl 2-dimethylbismuthanyl-2-methylpropanoate in tetrahydrofuran T=-78°C; 0.5 h; 2: iodobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 24 h;
参考文献
Kayahara, Eiichi; Yamada, Hiroto; Yamago, Shigeru
Chemistry - A European Journal, 2011 , vol. 17, # 19 p. 5272 - 5280
反应条件
silver hexafluoroantimonate 2 h; Ambient temperaturefurther reagent: Ag2CO3;
参考文献
Kimpe, Norbert De; Buyck, Laurent De; Verhe, Roland; Schamp, Niceas
Chemische Berichte, 1983 , vol. 116, # 11 p. 3631 - 3636
反应条件
potassium carbonate T=220°C; 6 h;
参考文献
Selva, Maurizio; Marques, Carlos Alberto; Tundo, Pietro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 10 p. 1323 - 1328