2-乙基-4,5-二甲基-1,3,2-二氧硼戊环合成路线 (共 3 条)
反应条件
in neat (no solvent)
byproducts: CH3NH2; mixt. heated, 70-150°C with stirring, under Ar, 9 h, CH3NH2 collected in H2SO4; distn. (vac.); elem. anal.;
参考文献
Koester, Roland; Seidel, Guenter; Boese, Roland; Wrackmeyer, Bernd
Chemische Berichte, 1990 , vol. 123, # 5 p. 1013 - 1028
反应条件
diethylboryl-pivalate
参考文献
Dahlhoff,W.V.; Koester,R.
Justus Liebigs Annalen der Chemie, 1975 , p. 1625 - 1636
反应条件
in neat (no solvent)
mixt. heated, 150°C;
参考文献
Koester, Roland; Seidel, Guenter; Boese, Roland; Wrackmeyer, Bernd
Chemische Berichte, 1990 , vol. 123, # 5 p. 1013 - 1028