(1-羟基-1-膦酰戊基)膦酸合成路线 （共 3 条）
反应条件
P4O6
heating; Yield given;
参考文献
Schuelke, Ulrich
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 51/52, p. 623 - 626
反应条件
1.1: CHCl3 / -10 - 0 °C
1.2: 95 percent / CH3OH / 1 h / 20 °C
2.1: 90 percent / CCl3COOH / 0.02 h / 25 °C
View Scheme
参考文献
Mallard, Isabelle; Benech, Jean-Marc; Lecouvey, Marc; Leroux, Yves
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 162, p. 15 - 23
反应条件
1: chloroform / 1 h / 20 °C
2: hydrogenchloride / water / 17 h / Reflux
View Scheme
参考文献
Seki, Masahiko
Synthesis, 2012 , vol. 44, # 10 p. 1556 - 1558
