1,1,3,4-四甲基-1-锗杂-3-环戊烯合成路线 (共 36 条)
反应条件
in cyclohexane
Irradiation (UV/VIS); Irradn. with a 110 W low-pressure Hg arc lamp at room temp. under Ar for 6 h.; GC-MS.;
参考文献
Mochida, Kunio; Kikkawa, Haruhiko; Nakadaira, Yasuhiro
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 9 p. 2772 - 2777
反应条件
in further solvent(s)
Irradiation (UV/VIS); 3-methylpentane glass matrix, 77 K; not sepd., detected by GC-MS;
参考文献
Sakurai, Hideki; Sakamoto, Kenkichi; Kira, Mitsuo
Chemistry Letters, 1984 , p. 1379 - 1382
反应条件
in cyclohexane
Irradiation (UV/VIS); irradiation of catenate in cyclohexane containing an excess of 2,3-dimethylbutadiene with a 110 W low pressure Hg arc lamp at room temp. under Ar for 1-4 h, further products; identification by GC and GC-MS;
参考文献
Mochida, Kunio; Kikkawa, Haruhiko; Nakadaira, Yasuhiro
Journal of Organometallic Chemistry, 1991 , vol. 412, # 1.2 p. 9 - 19
反应条件
in neat (no solvent)
pyrolysis at 470°C, ca. 2 Torr in presence of 10-fold excess of 2-methylbutadiene; GC at 90°C;
参考文献
Lei, Deqing; Gaspar, Peter P.
Polyhedron, 1991 , vol. 10, p. 1221 - 1226
反应条件
in not given
elem. anal.;
参考文献
Khabashesku, Valery N.; Boganov, Sergei E.; Kudin, Konstantin N.; Margrave, John L.; Nefedov, Oleg M.
Organometallics, 1998 , vol. 17, # 23 p. 5041 - 5051
反应条件
3-chloro-benzenecarboperoxoic acid in diethyl ether
参考文献
Manuel, Georges; Bertrand, Guy; Anba, Fatina El
Organometallics, 1983 , vol. 2, p. 391 - 394