(6-溴-1-氧己基)二茂铁合成路线 （共 2 条）
反应条件
aluminium trichloride in dichloromethane
modified method: K. Uosaki, et. al.Langmuir, 1991, 7, 1510; A. S. Viana,et. al. Phys. Chem. Chem. Phys., 2001, 3, 3411; C. J. Yu, et al. J. Org . Chem., 2001, 66, 2937; under N2, stirring for 4 h at room temp.; HCl was added, aq. phase was sepd. and extd. with CH2Cl2, organic layerswere collected, dried over MgSO4, evapd., chromd. (silica gel); MS;
参考文献
Lo, Kenneth Kam-Wing; Ng, Dominic Chun-Ming; Lau, Jason Shing-Yip; Wu, Rudolf Shiu-Sun; Lam, Paul Kwan-Sing
New Journal of Chemistry, 2003 , vol. 27, # 2 p. 274 - 279
反应条件
Al2O3; trifluoroacetic anhydride in neat (no solvent)
参考文献
Nyamori, Vincent O.; Gumede, Mhleli; Bala, Muhammad D.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 8 p. 1126 - 1132
