3,4-二氢苯并[a]蒽-1(2h)-酮合成路线 （共 15 条）
反应条件
1: diethyl ether / 0 °C
2: p-toluenesulfonic acid / benzene / 0.25 h / 50 °C
3: 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 3 h / Heating
View Scheme
参考文献
Nashed, Nashaat T.; Balani, Suresh K.; Loncharich, Richard J.; Sayer, Jane M.; Shipley, David Y.; Mohan, Ram S.; Whalen, Dale L.; Jerina, Donald M.
Journal of the American Chemical Society, 1991 , vol. 113, # 10 p. 3910 - 3919
反应条件
palladium; 1-methyl-naphthalene
参考文献
Fu,P.P. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 24 p. 4265 - 4271
反应条件
in diethyl ether
T=0°C;
参考文献
Nashed, Nashaat T.; Balani, Suresh K.; Loncharich, Richard J.; Sayer, Jane M.; Shipley, David Y.; Mohan, Ram S.; Whalen, Dale L.; Jerina, Donald M.
Journal of the American Chemical Society, 1991 , vol. 113, # 10 p. 3910 - 3919
反应条件
in diethyl ether
0 deg C to room temperature; room temperature, 12 h;
参考文献
Laali, Kenneth K.; Tanaka, Mutsuo
Journal of Organic Chemistry, 1998 , vol. 63, # 21 p. 7280 - 7285
反应条件
toluene-4-sulfonic acid; 3-hydroxy-2,2-dimethylpropanol in toluene
20 h; Reflux;
参考文献
Imai, Masao; Morais, Goreti Ribeiro; Al-Hindawi, Bassam; Al-Sulaibi, Mazen A.M.; Meetani, Mohammad; Thiemann, Thies
Journal of Chemical Research, 2010 , # 6 p. 325 - 329
