9-苄基-9-氮杂双环[3.3.1]壬烷合成路线 （共 4 条）
反应条件
hydrogen; palladium on activated charcoal; bis(η3-allyl-μ-chloropalladium(II)) in ethanol T=95°C; P=95000.1 Torr; 40 h;
参考文献
Hayashi, Tamio; Sawamura, Masaya; Ito, Yoshihiko
Tetrahedron, 1992 , vol. 48, # 11 p. 1999 - 2012
反应条件
potassium hydroxide; hydrazine hydrate in diethylene glycol
参考文献
Hayashi, Tamio; Sawamura, Masaya; Ito, Yoshihiko
Tetrahedron, 1992 , vol. 48, # 11 p. 1999 - 2012
反应条件
1: 98 percent / methanol / 72 h / Ambient temperature
2: 48 percent / 85percent aq. KOH, hydrazine hydrate / ethane-1,2-diol; H2O / a) 130-140 deg C, 2 h, b) 210 deg C, 6 h
View Scheme
参考文献
Nelsen, Stephen F.; Cunkle, Glen T.
Journal of Organic Chemistry, 1985 , vol. 50, # 20 p. 3701 - 3705
反应条件
1: 98 percent / methanol / 72 h / Ambient temperature
2: 48 percent / 85percent aq. KOH, hydrazine hydrate / ethane-1,2-diol; H2O / a) 130-140 deg C, 2 h, b) 210 deg C, 6 h
View Scheme
参考文献
Nelsen, Stephen F.; Cunkle, Glen T.
Journal of Organic Chemistry, 1985 , vol. 50, # 20 p. 3701 - 3705
