2-(2,5-二甲苯基)-2-羟基乙酸合成路线 (共 10 条)
参考文献
Savariau
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1908 , vol. 146, p. 298
反应条件
tin(IV) chloride
Erwaermen des Reaktionsprodukts mit wss. Kalilauge und Erwaermen der mit wss. Salzsaeure angesaeuerten Reaktionsloesung;
参考文献
Riebsomer et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 2080
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Riebsomer; Burkett
Proceedings of the Indiana Academy of Science, 1938 , vol. 48, p. 77
反应条件
sodium hydroxide in 1,4-dioxane
T=95 - 100°C;
参考文献
Bal'on, Ya. G.; Smirnov, V. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 12.1 p. 2249 - 2254
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 12 p. 2507 - 2513
反应条件
sodium hydroxide in 1,4-dioxane
T=95 - 100°C;
参考文献
Bal'on, Ya. G.; Smirnov, V. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 12.1 p. 2249 - 2254
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 12 p. 2507 - 2513
反应条件
sodium hydroxide in 1,4-dioxane
T=95 - 100°C;
参考文献
Bal'on, Ya. G.; Smirnov, V. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 12.1 p. 2249 - 2254
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 12 p. 2507 - 2513
反应条件
sodium hydroxide in 1,4-dioxane
T=95 - 100°C;
参考文献
Bal'on, Ya. G.; Smirnov, V. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 12.1 p. 2249 - 2254
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 12 p. 2507 - 2513
反应条件
hydrogenchloride
Heating;
参考文献
Kamata, Kazuyuki; Terashima, Masanao
Journal of the Chemical Society, Chemical Communications, 1994 , # 24 p. 2771 - 2772
反应条件
1: 50percent NaOH, Bu4NBr / tetrahydrofuran
2: 65 percent / LDA / tetrahydrofuran / 3.5 h / -75 °C
3: 95 percent / 3 M HCl / Heating
View Scheme
参考文献
Kamata, Kazuyuki; Terashima, Masanao
Journal of the Chemical Society, Chemical Communications, 1994 , # 24 p. 2771 - 2772
反应条件
1: 65 percent / LDA / tetrahydrofuran / 3.5 h / -75 °C
2: 95 percent / 3 M HCl / Heating
View Scheme
参考文献
Kamata, Kazuyuki; Terashima, Masanao
Journal of the Chemical Society, Chemical Communications, 1994 , # 24 p. 2771 - 2772
参考文献
Savariau
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1908 , vol. 146, p. 298