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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
57680-77-0
合成路线
（共 12 条）
666-52-4
氘代丙酮
+
57680-77-0
→
反应条件
3732-31-8
1,1’-双金刚烷
+
281-23-2
金刚烷
+
768-95-6
1-金刚烷醇
+
114332-08-0
反应条件
in diethyl ether T=0°C; 15 h; Further byproducts given. Yields of byproduct given;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
666-52-4
氘代丙酮
+
57680-77-0
→
反应条件
3732-31-8
1,1’-双金刚烷
+
281-23-2
金刚烷
+
768-95-6
1-金刚烷醇
+
35332-48-0
+
114332-08-0
反应条件
in diethyl ether T=0°C; 0.25 h; without aceton-d6; several other aldehydes, ketones and acyl chlorides.; Product distribution;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
666-52-4
氘代丙酮
+
57680-77-0
→
反应条件
3732-31-8
1,1’-双金刚烷
+
281-23-2
金刚烷
+
768-95-6
1-金刚烷醇
+
114332-08-0
反应条件
in diethyl ether T=0°C; 15 h; Further byproducts given. Yields of byproduct given;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
666-52-4
氘代丙酮
+
57680-77-0
→
反应条件
3732-31-8
1,1’-双金刚烷
+
281-23-2
金刚烷
+
768-95-6
1-金刚烷醇
+
35332-48-0
+
114332-08-0
反应条件
in diethyl ether T=0°C; 0.25 h; without aceton-d6; several other aldehydes, ketones and acyl chlorides.; Product distribution;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
57680-77-0
+
67-64-1
丙酮
→
反应条件
775-64-4
2-(1-金刚烷基)-2-丙醇
反应条件
in diethyl ether T=0°C; 15 h;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
57680-77-0
→
反应条件
665-66-7
盐酸金刚烷胺
反应条件
1: With N,N,N',N',N'',N''-hexamethylphosphoric triamide; CuCN*LiCl; 4,4'-bis(4-trifluoromethyl)benzophenone O-methylsulfonyloxime in tetrahydrofuran T=0°C; Substitution; 1 h; 2: With hydrogenchloride in water; acetone T=25°C; Hydrolysis; 0.5 h;
参考文献
Tsutsui, Hironori; Ichikawa, Tomoko; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 8 p. 1869 - 1878
57680-77-0
+
75-36-5
乙酰氯
→
反应条件
1660-04-4
1-金刚烷甲酮
反应条件
copper(I) bromide in diethyl ether T=-5°C; 1 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, , vol. 23, # 5 p. 970 - 976
57680-77-0
+
141-78-6
乙酸乙酯
→
反应条件
1660-04-4
1-金刚烷甲酮
反应条件
in diethyl ether T=0°C; 0.25 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, , vol. 23, # 5 p. 970 - 976
106-38-7
对溴甲苯
+
57680-77-0
→
反应条件
1459-55-8
对(1-金刚烷)甲苯
反应条件
1: 1-AdMgBr With bis(acetylacetonate)nickel(II); 1-(2-carboxyethyl)-3-mesityl-1H-imidazol-3-ium chloride; lithium tert-butylate in tetrahydrofuran; diethyl ether T=0°C; 0.166667 h; Inert atmosphere; 2: para-bromotoluene in tetrahydrofuran; diethyl ether T=0 - 20°C; Kumada-Corriu-Tamao type reaction; Inert atmosphere;
参考文献
Lohre, Claudia; Droege, Thomas; Wang, Congyang; Glorius, Frank
Chemistry - A European Journal, 2011 , vol. 17, # 22 p. 6052 - 6055
666-52-4
氘代丙酮
+
57680-77-0
→
反应条件
3732-31-8
1,1’-双金刚烷
+
281-23-2
金刚烷
+
768-95-6
1-金刚烷醇
+
114332-08-0
反应条件
in diethyl ether T=0°C; 15 h; Further byproducts given. Yields of byproduct given;
参考文献
Yurchenko, A. G.; Fedorenko, T. V.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 875 - 880
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 970 - 976
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