5-丙基-5H-呋喃-2-酮合成路线 (共 7 条)
反应条件
baker's yeast stereochemical outcome investigated; also other homologues; Product distribution;
参考文献
Fronza, Giovanni; Fuganti, Claudio; Grasselli, Piero; Mele, Andrea; Sarra, Antonella; Allegrone, Gianna; Barbeni, Massimo
Tetrahedron Letters, 1993 , vol. 34, # 40 p. 6467 - 6470
反应条件
(PM,RS,RS)-i-Pr-SPRIX; palladium diacetate; p-benozquinone in 1,2-dichloro-ethane
T=30°C; 12 h; Inert atmosphere;
参考文献
Bajracharya, Gan B.; Koranne, Priti S.; Nadaf, Rashid N.; Gabr, Randa Kassem Mohamed; Takenaka, Kazuhiro; Takizawa, Shinobu; Sasai, Hiroaki
Chemical Communications, 2010 , vol. 46, # 47 p. 9064 - 9066
反应条件
silver trifluoroacetate in dichloromethane
T=-78 - 20°C; 4 h;
参考文献
Jefford, Charles W.; Sledeski, Adam W.; Boukouvalas, John
Journal of the Chemical Society, Chemical Communications, 1988 , # 5 p. 364 - 365
反应条件
1: 34 percent / triethylamine / CH2Cl2 / -78 deg C, 6 h then 20 deg C, 12 h
2: W-2 Raney nickel / acetone / 7 h / Heating
View Scheme
参考文献
Gill, G. Bryon; Idris, Muhammad Sum Hj.
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4811 - 4814
反应条件
W-2 Raney nickel in acetone
7 h; Heating; Yield given;
参考文献
Gill, G. Bryon; Idris, Muhammad Sum Hj.
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4811 - 4814
反应条件
Amberlyst A-21 in ethyl acetate
24 h;
参考文献
Ma, Jie; Wang, Si Hong; Guan, Rong Tian
Synthetic Communications, 2006 , vol. 36, # 9 p. 1229 - 1233
反应条件
acetic anhydride
1 h; Heating;
参考文献
Sedavkina, V. A.; Morozova, N. A.; Egorova, A. Yu.; Ostroumov, I. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 4 p. 377 - 380
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 4 p. 451 - 454