N,N-双(苯基甲基)-1H-苯并噻唑-1-甲胺合成路线 (共 6 条)
反应条件
sodium tetrahydroborate in tetrahydrofuran Ambient temperature;
参考文献
Katritzky, Alan R.; Yannakopoulou, Konstantina; Lue, Ping; Rasala, Danuta; Urogdi, Laszlo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 225 - 233
反应条件
in tetrahydrofuran; diethyl ether 1 h; Heating;
参考文献
Katritzky, Alan R.; Yannakopoulou, Konstantina; Lue, Ping; Rasala, Danuta; Urogdi, Laszlo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 225 - 233
反应条件
in ethanol
T=20°C; 24.0833 h;
参考文献
TAKEDA PHARMACEUTICAL COMPANY LIMITED; CAO, Sheldon X.; ICHIKAWA, Takashi; KIRYANOV, Andre, A.; MCBRIDE, Christopher; NATALA, Srinivasa, Reddy; KALDOR, Stephen, W.; STAFFORD, Jeffrey, A.
Patent: WO2010/25073 A1, 2010 ;
Location in patent: Page/Page column 17-20 ;
WO 2010/025073 A1
反应条件
1.) methanol, water, 7 h, 2.) Et2O, reflux, overnight;
参考文献
Katritzky, Alan R.; Yannakopoulou, Konstantina; Lue, Ping; Rasala, Danuta; Urogdi, Laszlo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 225 - 233
反应条件
in tetrahydrofuran; diethyl ether
1 h; Heating;
参考文献
Katritzky, Alan R.; Yannakopoulou, Konstantina; Lue, Ping; Rasala, Danuta; Urogdi, Laszlo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 225 - 233
反应条件
in tetrahydrofuran; diethyl ether
1 h; Heating;
参考文献
Katritzky, Alan R.; Yannakopoulou, Konstantina; Lue, Ping; Rasala, Danuta; Urogdi, Laszlo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 225 - 233