苯乙酮乙烷-1,2-二基二硫代缩醛合成路线 （共 34 条）
反应条件
Envirocat EPZ10R in dichloromethane
4 h; Heating;
参考文献
Gajare; Shingare; Bandgar
Journal of Chemical Research - Part S, 1998 , # 8 p. 452 - 453
反应条件
di-n-butylbis(trifluoromethanesulfonyloxy)stannane in 1,2-dichloro-ethane
T=35°C; 20 h;
参考文献
Sato, Tsuneo; Otera, Junzo; Nozaki, Hitosi
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4971 - 4978
反应条件
di-n-butylbis(trifluoromethanesulfonyloxy)stannane in 1,2-dichloro-ethane
T=35°C; 1 h;
参考文献
Sato, Tsuneo; Otera, Junzo; Nozaki, Hitosi
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4971 - 4978
反应条件
1: 100 percent / H2O / Nafion-H / acetone / 0.5 h
2: 96 percent / Nafion-H / benzene / Heating
View Scheme
参考文献
Olah, George A.; Narang, Subhash C.; Meidar, David; Salem, George F.
Synthesis, 1981 , # 4 p. 282 - 283
反应条件
mercury dichloride
24 h; Heating;
参考文献
Jo, Shigeo; Tanimoto, Shigeo; Oida, Tatsuo; Okano, Masaya
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 5 p. 1434 - 1436
反应条件
1: 83 percent / (bromodimethyl)sulfonium bromide; triethyl orthoformate / 0.17 h / 20 °C
2: 90 percent / (bromodimethyl)sulfonium bromide / 0.25 h / 20 °C
View Scheme
参考文献
Khan, Abu T.; Mondal, Ejabul; Ghosh, Subrata; Islam, Samimul
European Journal of Organic Chemistry, 2004 , # 9 p. 2002 - 2009
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene
16 h; Heating; Yield given. Yields of byproduct given;
参考文献
Ni, Zhi-Jie; Luh, Tien-Yau
Journal of the Chemical Society, Chemical Communications, 1988 , # 15 p. 1011 - 1012
反应条件
1: 85 percent / 85percent 3-Cl-C6H4-COOOH / CH2Cl2 / -20 °C
2: 44 percent / KMnO4 / MgSO4, Me(C8H17)3N(+)Cl(-) / CH2Cl2; H2O / Ambient temperature
3: 38 percent / diethyl ether; hexane / Ambient temperature
View Scheme
参考文献
Schaumann, Ernst; Ruehter, Gerd
Chemische Berichte, 1988 , vol. 121, p. 1159 - 1164
反应条件
lithium diisopropyl amide
1.) THF, -15 deg C, 1 h, 2.) THF, a) -10 to -5 deg C, b) RT, 24 h; Yield given. Multistep reaction;
参考文献
Ikehira, Hideyuki; Tanimoto, Shigeo; Oida, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2537 - 2538
反应条件
lithium diisopropyl amide
1.) THF, -15 deg C, 1 h, 2.) THF, a) -10 to -5 deg C, b) RT, 24 h; Yield given. Multistep reaction;
参考文献
Ikehira, Hideyuki; Tanimoto, Shigeo; Oida, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 8 p. 2537 - 2538
