苯乙酮乙烷-1,2-二基二硫代缩醛合成路线 （共 34 条）
反应条件
dihydrogen peroxide in acetic acid
T=60 - 70°C; 8 h;
参考文献
Love; Chao
Synthetic Communications, 1993 , vol. 23, # 21 p. 3073 - 3079
反应条件
tungsten hexachloride; dimethyl sulfoxide in dichloromethane
0.5 h; Ambient temperature;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Karimi, Babak
Synlett, 1999 , # 4 p. 413 - 414
反应条件
1.1: tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 88 percent / tetrahydrofuran; hexane / 20 °C
2.1: 63 percent / Fe(acac)3; MeMgI / toluene; diethyl ether / Heating
View Scheme
参考文献
Huang, Li-Fu; Chen, Chih-Wei; Luh, Tien-Yau
Organic Letters, 2007 , vol. 9, # 18 p. 3663 - 3665
反应条件
potassium superoxide; tetraethylammonium bromide in N,N-dimethyl-formamide
T=20°C;
参考文献
Shukla, Ajay Kumar; Verma, Manjusha; Singh, Krishna Nand
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 8 p. 1748 - 1752
