3-甲氧基-4-丙氧基苯甲醛合成路线 （共 11 条）
反应条件
potassium iodide; potassium carbonate in N,N-dimethyl-formamide
参考文献
US2003/186943 A1, ;
US6458829 B1, ;
反应条件
potassium carbonate in acetone Reflux;
参考文献
Chemical Biology and Drug Design, , vol. 78, # 1 p. 101 - 111
反应条件
1: potassium carbonate; potassium iodide / ethanol / 10 h / |Reflux 2: trichlorophosphate / 19 h / 100 - 115 °C / |Cooling with ice View Scheme
参考文献
Research on Chemical Intermediates, , vol. 39, # 6 p. 2849 - 2856
反应条件
trichlorophosphate T=100 - 115°C; Vilsmeier-Haack Formylation; 19 h; Cooling with ice; Overall yield = 81.8 percent; Overall yield = 6.3 g;
参考文献
Research on Chemical Intermediates, , vol. 39, # 6 p. 2849 - 2856
参考文献
Monatshefte fuer Chemie, , vol. 77, p. 54
参考文献
Journal of the Chemical Society, , p. 1892
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 5 h;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
potassium permanganate
参考文献
Pearl
Journal of the American Chemical Society, 1955 , vol. 77, p. 757
反应条件
sodium tetrahydroborate in ethanol; water
参考文献
Inflazyme Pharmaceuticals Ltd.
Patent: US2003/186943 A1, 2003 ;
Title/Abstract Full Text Show Details
Inflazyme Pharmaceuticals Ltd.
Patent: US6458829 B1, 2002 ;
参考文献
Inflazyme Pharmaceuticals Ltd.
Patent: US6770658 B2, 2004 ;
