(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in toluene Suzuki-Miyaura reaction; 24 h; Heating;
参考文献
Cammidge, Andrew N.; Goddard, Victoria H. M.; Gopee, Hemant; Harrison, Nicola L.; Hughes, David L.; Schubert, Christopher J.; Sutton, Benjamin M.; Watts, Gary L.; Whitehead, Andrew J.
Organic Letters, 2006 , vol. 8, # 18 p. 4071 - 4074
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; toluene / 5 h / |Reflux 2: anhydrous iron chloride; bromine / tetrachloromethane / 12 h / 0 - 20 °C 3: diethylphosphoric acid ethyl ester / 7 h / 150 °C View Scheme
参考文献
ROHM AND HAAS ELECTRONIC MATERIALS KOREA LTD.; NA, Hong-Yoep; KIM, Chi-Sik; KU, Jong-Seok; KWON, Hyuck-Joo; LEE, Kyung-Joo; KIM, Bong-Ok
Patent: WO2013/162284 A1, 2013 ;