甲基2-羟基-4,6-二甲基-苯甲酸酯合成路线 (共 4 条)
反应条件
titanium tetrachloride in dichloromethane
T=-78 - 20°C;
参考文献
Reim, Stefanie; Lau, Matthias; Langer, Peter
Tetrahedron Letters, 2006 , vol. 47, # 38 p. 6903 - 6905
反应条件
1: With titanium tetrachloride in dichloromethane
T=-78 - 20°C; 18.5 h; Inert atmosphere;
2: With hydrogenchloride in dichloromethane; water
参考文献
Reim, Stefanie; Lau, Matthias; Adeel, Muhammad; Hussain, Ibrar; Yawer, Mirza A.; Riahi, Abdolmajid; Ahmed, Zafar; Fischer, Christine; Reinke, Helmut; Langer, Peter
Synthesis, 2009 , # 3 p. 445 - 463
反应条件
titanium tetrachloride; triethylamine
1.) hexane, 2.) dichloromethane, -78 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Chan, Tak-Hang; Brownbridge, Peter
Journal of the American Chemical Society, 1980 , vol. 102, # 10 p. 3534 - 3538
参考文献
Friedrichsen,W.
Justus Liebigs Annalen der Chemie, 1975 , p. 1545 - 1562