1,10-邻二氮杂菲-2,9-二甲酸合成路线 （共 8 条）
反应条件
1: SeO2 / dioxane / 2 h / Heating 2: 430 mg / aq. HNO3 / 2 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 7 p. 1856 - 1857
反应条件
nitric acid 4 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 31, # 1 p. 1 - 10
反应条件
sulfuric acid T=80 - 90°C; 6 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 75 - 82
反应条件
nitric acid 3 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 18, p. 599 - 602
反应条件
hydrogenchloride
2.5 h; Heating;
参考文献
Chandler, Christopher J.; Deady, Leslie W.; Reiss, James A.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 599 - 602
反应条件
1: 98 percent / pyridine; dimethylformamide / 12 h / 20 °C
2: NaBH4 / 1,2-dimethoxy-ethane / 8 h / 20 °C
View Scheme
参考文献
Esposito, Veronica; Galeone, Aldo; Mayol, Luciano; Oliviero, Giorgia; Randazzo, Antonio; Varra, Michela
European Journal of Organic Chemistry, 2002 , # 24 p. 4228 - 4233
反应条件
1: 98 percent / pyridine; dimethylformamide / 12 h / 20 °C
2: NaBH4 / 1,2-dimethoxy-ethane / 8 h / 20 °C
3: 95 percent / pyridine / 8 h
4: 54 percent / aq. HBr / 2 h / Heating
View Scheme
参考文献
Esposito, Veronica; Galeone, Aldo; Mayol, Luciano; Oliviero, Giorgia; Randazzo, Antonio; Varra, Michela
European Journal of Organic Chemistry, 2002 , # 24 p. 4228 - 4233
参考文献
Smith, David J.; Blake, Alexander J.; Wilson, Claire; Champness, Neil R.
Dalton Transactions, 2011 , vol. 40, # 45 p. 12257 - 12264
