1,10-菲啰啉-2,9-二甲醛合成路线 (共 7 条)
反应条件
nitric acid 4 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 31, # 1 p. 1 - 10
反应条件
selenium(IV) oxide in 1,4-dioxane; water
2 h; Reflux;
参考文献
Adam, Rosa; Ballesteros-Garrido, Rafael; Vallcorba, Oriol; Abarca, Belen; Ballesteros, Rafael; Leroux, Frederic R.; Colobert, Francoise; Amigo, Jose M.; Rius, Jordi
Tetrahedron Letters, 2013 , vol. 54, # 32 p. 4316 - 4319
参考文献
Smith, David J.; Blake, Alexander J.; Wilson, Claire; Champness, Neil R.
Dalton Transactions, 2011 , vol. 40, # 45 p. 12257 - 12264
反应条件
oxygen; thiamine chloride hydrochloride; triethylamine
3 h; Reflux;
参考文献
Goswami, Shyamaprosad; Hazra, Anita
Chemistry Letters, 2009 , vol. 38, # 5 p. 484 - 485
反应条件
1: 61 percent / 80percent HNO3 / 3 h / Heating
2: 67 percent / HCl(g) / 2.5 h / Heating
View Scheme
参考文献
Chandler, Christopher J.; Deady, Leslie W.; Reiss, James A.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 599 - 602
反应条件
sodium tetrahydroborate
Reduction; 4 h; Heating;
参考文献
Shaul, Mazi; Cohen, Yoram
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9358 - 9364
反应条件
1: 68 percent / NaBH4 / ethanol / 2 h / Heating
2: 79 percent / 48percent HBr / 2 h / Heating
View Scheme
参考文献
Chandler, Christopher J.; Deady, Leslie W.; Reiss, James A.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 599 - 602