1: 4-iodophenyl triflate With isopropylmagnesium chloride in tetrahydrofuran
T=-20°C;
2: trifluoromethanesulfonic anhydride Further stages.;
参考文献
Herbert, John M.; Kohler, Andrew D.; Le Strat, Franck; Whitehead, David
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 440 - 441
Herbert, John M.; Kohler, Andrew D.; Le Strat, Franck; Whitehead, David
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 440 - 441
1: NIS; sulfuric acid / 20 °C
2: 35 percent / i-PrMgCl / tetrahydrofuran / -20 °C
View Scheme
参考文献
Herbert, John M.; Kohler, Andrew D.; Le Strat, Franck; Whitehead, David
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 440 - 441