(S)-(+)-1,2-二苯乙醇合成路线 (共 35 条)
反应条件
Lipase PS-C II in decane
T=80°C; 3 h; Enzymatic reaction; Title compound not separated from byproducts;
参考文献
Ema, Tadashi; Kageyama, Masafumi; Korenaga, Toshinobu; Sakai, Takashi
Tetrahedron Asymmetry, 2003 , vol. 14, # 24 p. 3943 - 3947
反应条件
tetraproline chiral stationary phase packed on HPLC column in hexane; isopropyl alcohol
Resolution of racemate;
参考文献
Dai, Zhi; Ye, Guozhong; Pittman Jr., Charles U.; Li, Tingyu
Chirality, 2012 , vol. 24, # 4 p. 329 - 338
反应条件
chromyl nitrate in tetrachloromethane; dichloromethane
reaction conditions: -78 deg C (1 h), room temperature (1 h); effects of solvents; competition with styrene in acetone; relative reactivity; Product distribution;
参考文献
Miyaura, N.; Kochi, J. K.
Journal of the American Chemical Society, 1983 , vol. 105, # 8 p. 2368 - 2378
参考文献
Curtin; Leskowitz
Journal of the American Chemical Society, 1951 , vol. 73, p. 2630,2632
参考文献
Kharasch; Clapp
Journal of Organic Chemistry, 1938 , vol. 3, p. 355,359