2-溴-1-(5-氯噻吩-2-基)乙酮合成路线 (共 2 条)
反应条件
copper(ll) bromide in chloroform; ethyl acetate 53 h; Inert atmosphere;
参考文献
Salonen, Laura M.; Holland, Mareike C.; Kaib, Philip S. J.; Haap, Wolfgang; Benz, Joerg; Mary, Jean-Luc; Kuster, Olivier; Schweizer, W. Bernd; Banner, David W.; Diederich, Francois
Chemistry - A European Journal, 2012 , vol. 18, # 1 p. 213 - 222
反应条件
in DMF (N,N-dimethyl-formamide) T=5 - 20°C; 18.5 h; UV-irradiation;
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2004/11410 A1, 2004 ;
Location in patent: Page 83 ;
WO 2004/011410 A1