6-碘-1,4-苯并二氧烷合成路线 （共 7 条）
反应条件
1: With hydrogenchloride; sodium nitrite in water T=0°C; 0.416667 h; 2: With urea in water 0.25 h; 3: With potassium iodide in dichloromethane; water T=20°C;
参考文献
SLOAN-KETTERING INSTITUTE FOR CANCER RESEARCH; CHIOSIS, Gabriela; TALDONE, Tony; SUN, Weilin
Patent: WO2011/44394 A1, 2011 ;
Location in patent: Page/Page column 110 ;
反应条件
iodine; periodic acid in ethanol 0.75 h; Heating;
参考文献
Sosnowski, Maciej; Skulski, Lech
Molecules, 2005 , vol. 10, # 2 p. 401 - 406
反应条件
[bis(acetoxy)iodo]benzene; iodine in 1,2-dichloro-ethane T=60 - 70°C; Irradiation;
参考文献
Tetrahedron Letters, , vol. 37, # 14 p. 2441 - 2444
反应条件
[bis(acetoxy)iodo]benzene; iodine in 1,2-dichloro-ethane T=60 - 70°C; 2 h; Irradiation;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 5 p. 787 - 793
反应条件
1: With copper(l) iodide; caesium carbonate; L-proline in dimethyl sulfoxide T=130°C; Ullmann type reaction; 24 h; Inert atmosphere; 2: in dimethyl sulfoxide T=140°C; 12 h; 3: With hydrogenchloride in water pH=2 - 3;
参考文献
Yang, Daoshan; Yang, Haijun; Fu, Hua
Chemical Communications, 2011 , vol. 47, # 8 p. 2348 - 2350
反应条件
N-iodo-succinimide; CF3COOH in acetonitrile
参考文献
Cai, Xiong; Qian, Changgeng
Patent: US2010/184801 A1, 2010 ;
反应条件
alpha-hydroxyethanoic acid; Cu(OH)2; sodium hydroxide in water; dimethyl sulfoxide T=120°C; 6 h; Inert atmosphereSchlenk technique;
参考文献
Xiao, Yan; Xu, Yongnan; Cheon, Hwan-Sung; Chae, Junghyun
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5804 - 5809
