4-(吡啶-2-甲氧基)苯甲醛合成路线 （共 3 条）
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=50°C;
参考文献
Pharma Eight Co. Ltd; SUGIMOTO, Hachiro; OKUDA, Michiaki; TAKAHASHI, Takashi; HIJIKURO, Ichiro; SUZUKI, Hidetaka; NAKAYAMA, Shinichi
Patent: EP2698368 A1, 2014 ;
Location in patent: Paragraph 0094 ;
反应条件
potassium hydroxide
1) DMSO, 1 h, 2) r.t., overnight; Yield given. Multistep reaction;
参考文献
Sundberg; Dahlhausen; Manikumar; Mavunkel; Biswas; Srinivasan; King Jr.; Waid
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 1 p. 129 - 137
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran; toluene
T=0 - 25°C;
参考文献
Wu, Ying; Tai, Hsin-Hsiung; Cho, Hoon
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 4 p. 1428 - 1433
