phosphorus tribromide in N,N-dimethyl-formamide
T=20°C; 0.5 h;
参考文献
Margolis, Brandon J.; Long, Kimberly A.; Laird, Dana L. T.; Ruble, J. Craig; Pulley, Shon R.
Journal of Organic Chemistry, 2007 , vol. 72, # 6 p. 2232 - 2235
1.1: HC(OEt)3 / 145 °C
1.2: 50 - 145 °C
1.3: diphenyl ether / 250 °C
2.1: 59 percent / PBr3 / dimethylformamide / 0.5 h / 20 °C
View Scheme
参考文献
Margolis, Brandon J.; Long, Kimberly A.; Laird, Dana L. T.; Ruble, J. Craig; Pulley, Shon R.
Journal of Organic Chemistry, 2007 , vol. 72, # 6 p. 2232 - 2235
