苄基 2,3,4-三-O-苄基-alpha-D-吡喃甘露糖苷合成路线 （共 12 条）
反应条件
sulfuric acid in methanol T=20°C;
参考文献
Fokt, Izabela; Skora, Stanislaw; Conrad, Charles; Madden, Timothy; Emmett, Mark; Priebe, Waldemar
Carbohydrate Research, 2013 , vol. 368, p. 111 - 119
反应条件
acetic acid in ethanol T=80°C;
参考文献
Doores, Katie J.; Fulton, Zara; Hong, Vu; Patel, Mitul K.; Scanlan, Christopher N.; Wormald, Mark R.; Finn; Burton, Dennis R.; Wilson, Ian A.; Davis, Benjamin G.
Proceedings of the National Academy of Sciences of the United States of America, 2010 , vol. 107, # 40 p. 17107 - 17112
反应条件
borane-THF; trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Daragics, Katalin; Fuegedi, Peter
Tetrahedron Letters, 2009 , vol. 50, # 24 p. 2914 - 2916
反应条件
1: 74 percent / NaH / dimethylformamide / 15 h 2: 45 percent / LiAlH4; AlCl3 / CH2Cl2; diethyl ether / Heating View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 24 p. 3938 - 3944
反应条件
1: 74 percent / NaH / dimethylformamide / 15 h 2: 45 percent / LiAlH4; AlCl3 / CH2Cl2; diethyl ether / Heating View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 24 p. 3938 - 3944
反应条件
1: 85 percent / pyridine, 4-dimethylaminopyridine / 72 h / 40 °C 2: sodium hydroxide / dimethylsulfoxide / 1.5 h / Ambient temperature 3: trifluoroacetic acid / dioxane; methanol / Heating View Scheme
参考文献
Carbohydrate Research, , vol. 150, p. 163 - 172
反应条件
1: sodium hydroxide / dimethylsulfoxide / 1.5 h / Ambient temperature 2: trifluoroacetic acid / dioxane; methanol / Heating View Scheme
参考文献
Carbohydrate Research, , vol. 150, p. 163 - 172
反应条件
1: 66 percent / acetyl chloride / 0 deg C, RT, 4 d 2: 85 percent / pyridine, 4-dimethylaminopyridine / 72 h / 40 °C 3: sodium hydroxide / dimethylsulfoxide / 1.5 h / Ambient temperature 4: trifluoroacetic acid / dioxane; methanol / Heating View Scheme
参考文献
Carbohydrate Research, , vol. 150, p. 163 - 172
反应条件
1: trimethylsilyltrifluoromethane sulfonate / CH2Cl2 / 1 h / -65 °C 2: CH3ONa, CH3OH / 2 h View Scheme
参考文献
Carbohydrate Research, , vol. 282, # 1 p. 101 - 111
反应条件
1: 66 percent / acetyl chloride / 0 deg C, RT, 4 d 2: 85 percent / pyridine, 4-dimethylaminopyridine / 72 h / 40 °C 3: sodium hydroxide / dimethylsulfoxide / 1.5 h / Ambient temperature 4: trifluoroacetic acid / dioxane; methanol / Heating View Scheme
参考文献
Carbohydrate Research, , vol. 150, p. 163 - 172
